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The rest of supernatant was diluted with deionized water (1:1, v / v ) to make the final sample prior to HPLC-TLS, HPLC-DAD or HPLC-ESI-MS analysis

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The hyper pigmentation has already lightened significantly

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Because these findings are largely based on laboratory and animal studies, expected outcomes in humans are uncertain and may vary by individual, dose, and the underlying condition